Download Compendium of Organic Synthetic Methods Volume 11 by Michael B. Smith PDF

By Michael B. Smith

Compendium of natural artificial tools, quantity eleven maintains the inducement of the sequence, that is to facilitate the quest for caliber, chosen useful crew differences, prepared via reacting useful workforce of beginning fabric and practical team shaped, with complete references to every response.

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Compendium of Organic Synthetic Methods Volume 11

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2000, 2191. ; NaBH4, SiOz ,rt , 10 min LPhCH20H Org. Prep. Proceed. , 2000, 32, 596. Bu3SnH ,MeOH -CHO Ph ~. ; Wada. M. , 1999, 40, 9059. ; i-PiOH ,225"C, 1 d * PhCHzOH 92% t PhCH,OII 90% Chem. , 1999, 281. ; Sandhu. S. Chem. , I999, 995. ; Swami. S. Synth. , I999, 29, 2129. PhCHO P hCI I 0 1 . SnC12-2 IIzO, Mg , THF 2. ; PhCHzOH Chakraborty, V. Synth. , 1999, 2Y, 2501. 90% 90% H Section 34B 21 Alcohols from Aldehydes ALKYLATION OF ALDEHYDES, FORMING ALCOHOLS SECTION 34R: ASYMMETRIC ALKYLATIONS Ti(Oi-Pr), , TIIF , AlEt3 PhCHO * tE' chiral sulfonated amino Ph alcohol ligand , 0°C You, 1 .

J. Chern. Rex (S), 2001, 54. ; Org. , 2001, 3, 2745. ee. -G. Syntett, 2001, 1956. ; Cha. K. , 2001, 42, 2059. T i c k ,Li , THF , rt OTs 18 h * +OH Synthesis, 2000, 1575. ; Nair. G. Synth. , 2000, 30, 313. ; s CeC13-7 HzO-NaI MeCN,6h ' * B 75% 76% Et n \O O/ O H 95% Synth. , 2000, 30, 3829. ; Furukawa, I. , 1999, 40, 6963. -S. Synth. , 1999, ZY, 2875. ; Okamoto, T. Synlcitt, 1999, 1636. c&ori 98% Section 39 Alcohols from Ethers SECTION 39: 45 ALCOHOLS AND THIOLS FROM ETHERS, EPOXIDES AND THIOETHERS Et3Al, 5% Pl'h3, toluene * D O rt,ld H '%It 99% Et Schneider.

Pornet. I. Synth. , 1999, 2Y, 3329. EtCHO 54% REVIEWS: "Catalytic Asymmetric Organic Zinc Addition to Carbonyl Compounds", Chem. , 2001, 101, 757. -B. ) occur in the literature. For reactions of the type RH 4 ROH (R = alkyl or aryl) see Section 41 (Alcohols and Phenols from IIydrides). SECTION 36: ALCOHOLS AND THIOLS FROM AMIDES NO ADDITIONAL EXAMPLES SECTION 37: ALCOHOLS AND THIOIS FROM AMINES 1. B uLi ,THF ,-45°C 2. H+ Me Me 3. 4. J. Org. ,2001, 42, 8007. 2 eqIn, H20 Ph . ; Ohfune, Y. , 2001, 42, 9073.

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